X射线荧光光谱法测定燃料中硫各标准的
合并定量限PLOQ、重复性r及其典型值、再现性R及其典型值
标准 |
D7212 |
D7039 |
D7220 |
D2622 |
D4294 |
ISO20884 |
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对应国内标准 |
|
NB/SH/T0842 |
|
GB/T11140 |
GB/T17040 |
|
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PLOQ |
7 mg/kg |
3.2 mg ⁄kg |
3 mg/kg |
3 mg/kg |
16.0 mg ⁄kg |
5 mg/kg |
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Type |
ALL |
ALL |
ALL |
ALL |
Gasoline |
Diesel |
High Power |
ALL |
Gasoline |
Diesel |
ALL |
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r |
1.6196X 0.1 |
0.4998X0.54 |
0.6430X 0.504 |
0.1462X0.8015 |
0.5006X0.4377 |
0.1037X0.8000 |
0.08681X0.8383 |
0.4347X0.6446 |
1.6658X0.3300 |
1.4477X0.3661 |
1.7+0.0248 X |
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R |
3.7668X 0.1 |
0.7384X0.54 |
1.1121X0.504 |
0.4273X0.8015 |
1.4533X0.4377 |
0.3856X0.8000 |
0.3086X0.8383 |
1.9182X0.6446 |
8.9798X0.3300 |
7.1295X0.3661 |
1.9+0.1201 X |
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S, mg/kg |
r |
R |
r |
R |
r |
R |
r |
R |
r |
R |
r |
R |
r |
R |
r |
R |
r |
R |
r |
R |
r |
R |
1.0 |
|
|
|
|
|
|
|
|
|
|
|
|
0.09 |
0.31 |
|
|
|
|
|
|
|
|
3.0 |
|
|
|
|
1.1 |
1.9 |
0.4 |
1.1 |
|
|
|
|
|
|
|
|
|
|
|
|
|
|
3.2 |
|
|
0.9 |
1.4 |
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
5.0 |
|
|
1.2 |
1.8 |
1.4 |
2.5 |
0.5 |
1.6 |
1.01 |
2.94 |
|
|
0.33 |
1.19 |
|
|
|
|
|
|
1.8 |
2.5 |
8.0 |
2.0 |
4.6 |
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
10.0 |
2.0 |
4.7 |
1.7 |
2.6 |
2.1 |
3.5 |
0.9 |
2.7 |
1.37 |
3.98 |
|
|
0.60 |
2.13 |
|
|
|
|
|
|
1.9 |
3.1 |
11.0 |
|
|
|
|
|
|
|
|
|
|
0.71 |
2.63 |
|
|
|
|
|
|
|
|
|
|
15.0 |
2.1 |
4.9 |
2.2 |
3.2 |
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
16.0 |
|
|
|
|
|
|
|
|
|
|
|
|
|
|
2.6 |
11 |
|
|
|
|
|
|
20.0 |
2.2 |
5.1 |
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
25.0 |
2.2 |
5.2 |
2.8 |
4.2 |
3.3 |
5.6 |
1.9 |
5.6 |
2.05 |
5.95 |
1.36 |
5.06 |
1.28 |
4.58 |
3.4 |
15 |
4.8 |
26 |
|
|
3.3 |
5.6 |
50.0 |
|
|
4.1 |
6.1 |
4.6 |
8.0 |
3.4 |
9.8 |
|
|
|
|
2.31 |
8.20 |
5.4 |
24 |
|
|
6.0 |
30 |
4.6 |
8.0 |
70.0 |
|
|
|
|
|
|
|
|
3.21 |
9.33 |
|
|
|
|
|
|
|
|
|
|
|
|
100 |
|
|
6 |
9 |
6.5 |
11.3 |
5.9 |
17.1 |
|
|
4.13 |
15.35 |
4.12 |
14.66 |
8.5 |
37 |
7.6 |
41 |
7.8 |
38 |
6.5 |
11.3 |
250 |
|
|
10 |
15 |
10.4 |
18.0 |
|
|
|
|
|
|
|
|
|
|
|
|
|
|
10.4 |
18.0 |
500 |
|
|
14 |
21 |
14.7 |
25.2 |
21 |
62 |
|
|
15.0 |
55.6 |
15.9 |
56.5 |
24 |
105 |
13 |
70 |
14 |
69 |
14.7 |
25.2 |
942 |
|
|
|
|
20.3 |
35.1 |
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
1000 |
|
|
21 |
31 |
|
|
37 |
108 |
|
|
26.0 |
96.9 |
28.4 |
101.0 |
37 |
165 |
16 |
88 |
18 |
89 |
|
|
2000 |
|
|
30 |
45 |
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
2822 |
|
|
36 |
54 |
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
5000 |
|
|
|
|
|
|
135 |
394 |
|
|
|
|
109.5 |
389.3 |
105 |
465 |
|
|
|
|
|
|
5500 |
|
|
|
|
|
|
|
|
|
|
102 |
379 |
|
|
|
|
29 |
154 |
34 |
167 |
|
|
10000 |
|
|
|
|
|
|
235 |
687 |
|
|
|
|
196 |
696 |
165 |
727 |
|
|
|
|
|
|
46000 |
|
|
|
|
|
|
798 |
2333 |
|
|
|
|
704 |
2501 |
440 |
1943 |
|
|
|
|
|
|